Korean Institute of Surface Engineering

pISSN : 1225-8024 | eISSN : 3399-8403


공학

한국표면공학회지 (29권5호 525-531)

CRYSTALLINE PHASES AND HARDNESS OF (Ti$_{1-x}$Al$_{x}$)N COATINGS DEPOSITED BY REACTIVE SPUTTERING


Park, Chong-Kwan;Park, Joo-Dong;Oh, Tae-Sung;


Department of Metallurgy and Materials Science, Hong Ik University;

Abstract

(Ti1-xAlx)N films were deposited on high speed steel and silicon substrates by reactive sputtering in mixed $Ar-N_2$ discharges. Crystalline phases and microhardness of ($Ti_1_xAl_x$)N films were investigated with variation of the film composition and substrate RF bias voltage. With Al content x of about 0.6, crystalline phase of ( $Ti_1_xAl_x$N films was changed from single-phase NaCl structure to two phase mixture of NaCl and wurtzite structures: Microhardness of ($Ti_1_xAl_x$)N films was largely improved by applying RF bias voltage above 50 V during deposition. Hardness of ($Ti_1_xAl_x$)N films reached a maximum value for Al content x of about 0.4, and 1900 kg/$mm^2$ was obtained for 1$mu m$-thick ($Ti_{0.6}Al_{0.4}$)N films.

Keywords