Korean Institute of Surface Engineering

pISSN : 1225-8024 | eISSN : 3399-8403


공학

한국표면공학회지 (50권3호 212-218)

Preparation of Nano-sized MgxNiyZn1-x-yFe2O4 by Ultrasonic Wet-Magnetic Separation Method

초음파 습식 자기분류법을 이용한 MgxNiyZn1-x-yFe2O4 나노입자 제조

구문선;권혁주;최용;
Gu, Moon Sun;Kwon, Hyuk Joo;Choi, Yong;

단국대학교 신소재공학과;(주)한스코;
Department of Materials Science and Engineering, Dankook University;R&D Center, HANSCO;

DOI : 10.5695/JKISE.2017.50.3.212

Abstract

$Mg_xNi_yZn_{1-x-y}Fe_2O_4$ ferrite powders were prepared by self-propagating high temperature synthesis followed by classifying with an ultrasonic wet-magnetic separation unit to get high pure nano-sized particles. The $Mg_xNi_yZn_{1-x-y}Fe_2O_4$ ferrites were well formed by using several powders like iron, nickel oxide, zinc oxide and magnesium oxide at 0.1 MPa of oxygen pressure. The ultrasonic wet-magnetic separation of pre-mechanical milled ferrite powders resulted in producing the powders with average size of 800 nm. The addition of a surfactant during the wet-magnetic separation process improved productivity more than twice. The coercive force, maximum magnetization and residual magnetization of the $Mg_xNi_yZn_{1-x-y}Fe_2O_4$ nano-powders with 800 nm size were 3651 A/m, $53.92Am^2/kg$ and $4.0Am^2/kg$, respectively.

Keywords

Nano-powders;Surface treatment;Wet-magnetic separation;