공학
한국표면공학회지 (43권5호 243-247)
Effect of Solution Compositions on Properties of Ni-Fe Nano Thin Film and Wire Made by Electrodeposition Method
Electrodeposition법으로 제조한 Ni-Fe 나노박막 및 나노선의 특성에 미치는 용액 조성의 영향
구본급;
Koo, Bon-Keup;
한밭대학교 신소재공학부;
Division of Advanced Materials Engineering, Hanbat National University;
DOI : 10.5695/JKISE.2010.43.5.243
Abstract
The micro Vickers hardness and internal stress of Ni-Fe metal thin film synthesized by electrodeposition method at $25^{circ}C$ were studied as a function of bath composition, and surface microstructure and atomic compositions of thin films were investigated by SEM and EDS. And the shape change of $200;{AA}$ Ni-Fe nanowires made using anodic aluminum oxide(AAO) templates by electrodeposition method were observed by SEM as a function of ultrasonic treatment time and bath composition. The Fe deposition contents on the substrate non-linearly increased with Fe ion concentration over total metal ion concentration. In case of low Fe contents film, the grain size is smaller and denser than high Fe contents deposited films, and the micro Vickers hardness increased with Fe contents of electrodeposited films. These results affected the shape change of nanowire after ultrasonic treatments.
Keywords
Electrodeposition;Ni-Fe;Nanowire;Thin film;Stress;Templates;Microhardness;Ultrasonic treatment;